MBE Components, Oxygen Atom Beam Source OBS

OBS

Oxygen Atom Beam Source

OBS 40 Oxygen Atom Beam Source on DN40CF (O.D. 2.75") flange with aperture plate

O₂ dissociation up to more than 80%, depending on operation conditions
Atomic oxygen flux density up to 1x10¹⁵/cm² s
No high-energy particles and ions
Low power consumption
Integrated water cooling, low thermal load on other experimental equipment
Optional customized aperture

The Oxygen Atom Beam Source OBS is a thermal gas cracker that produces an ion-free oxygen gas beam, thus avoiding ion induced damage to the substrate. It features a very compact design and is easy to install and to operate.
In contrast to oxygen plasma sources based on HF or HV ionization of gas molecules, or gas sources heated by HV electron bombardment, the OBS is heated by a DC operated filament, which surrounds a long cracking tube.
Developed in collaboration with Dr. Karl Georg Tschersich of the Institute of Bio- and Nanosystems (formerly Institute of Thin Films and Interfaces) at Juelich Research, the OBS is an extensively tested and well characterized oxygen source.

The intensity of the source can be controlled by the flow rate of oxygen and the heating power. The heating power determines the temperature of the cracking tube. Operation temperatures up to 1700°C provide an efficient thermal cracking of O₂ molecules within the tube. The high purity cracking tube is the only part of the OBS directly exposed to the oxygen gas. It ejects a narrow angle distributed gas beam toward the specimen. The narrow beam of the OBS allows high atomic oxygen flux rates at the sample position, while keeping the O₂ background pressure of the chamber low as compared to plasma sources. Furthermore, the high cracking efficiency of up to 80%, which is available for low flux applications, reduces the chamber background pressure significantly as compared to ozone generators, with which the ozone concentration is limited to about 10-15%.		Grade of dissociation as a function of the gas flow for typical cracking tube temperatures of the OBS (values are calculated for thermodynamical equilibrium conditions)
Despite the high temperatures needed for thermal gas cracking, the thermal load on the chamber is negligible, due to the integrated water cooling and use of a small diameter aperture (optional). The following options are available: - Usually the gas flow is regulated by a UHV leak valve or a mass flow controller which allow switching on and off the atom flux within several seconds. Short exposures can be terminated by a shutter which attenuates the oxygen atom flux down to the detection level. - Oxygen atoms passing the sample and hitting the chamber walls can induce reactions detrimental to the experiment. A customized aperture is available which limits the solid angle of oxygen atom emission. Outside this angle no beam atoms could be detected by the QMA. Although tested so far with oxygen only, the source can be used as well as a radical beam source by decomposing other molecules at temperatures up to 1900°C.		Total flux of O-atoms leaving the cell orifice for different cell operation parameters (gas flow and tube temperature). A flux of about 1*10¹⁷ atoms/s corresponds to a typical deposition rate of 1 monolayer/s at a substrate distance of about 200mm

Application

The use of a long, slender cracking tube results in a narrow angle distribution of the atomic oxygen beam (typical FWHM: 10-30°) which makes the OBS ideally suited for medium and low gas flux applications (up to 0.1 sccm) on smaller sample sizes or long substrate distances.
Due to its highly efficient oxygen cracking mechanism and the resulting low gas load on the vacuum system, the OBS can likewise be applied in standard UHV, MBE, and ALD systems as a reliable, highly efficient and low cost source for atomic oxygen.

Typical applications for the OBS are:

Oxide layer deposition
The OBS allows precise layer deposition of oxide layers, due to the fast and easy control of the gas flow by shutter or UHV leak-valve.

Surface cleaning procedures
Atomic oxygen is used for removal of surface carbon contaminations.

Surface oxidation
In surface analysis applications as well as in ALD technology atomic oxygen is used for the preparation of well defined oxide surface layers.

Atomic spectroscopy of single atoms
The particle density of about 10¹¹ low energy O-atoms per cm³ near the cell exit allows a wide range of fundamental spectroscopic experiments on single O-atoms.

Several publications to OBS are listed in section References / List of Publications.

Gas Injection System
For optimized performance, we offer a complete gas injection system for atomic oxygen. The gas injection system is completely assembled and only an O₂ gas cylinder is required to start operation. A simple turbo molecular pump can be used to evacuate the O₂ gas line. The O₂ gas line and all-metal leak valve can be baked to 180°C. Alternatively, the gas injection system can be equipped with a mass flow controller (MFC) plus an all-metal valve instead of an all-metal UHV leak valve. A mass flow controller in the gas line is preferred when the OBS is used primarily for high intensity, long term runs, where mass flow controllers require less attention due to their automated operation compared to the gas feed setup above. There are many different mass flow controllers on the market. It is recommended that the customer provide the MFC. The maximum system bake-out temperature depends on the specification of the MFC used.
fully UHV compatible O₂ gas cracking cell all-metal UHV leak valve / mass flow controller (MFC) plus all-metal valve for shut-off during MFC maintenance all-metal valve for gas feed evacuation O₂ gas purifier flexible UHV tube 1m max. length bakeable system O₂ bottle and stainless steel gas pressure reducing regulator (not included)	Gas injection system with all-metal leak valve. In the alternative design with mass flow controller (MFC), the all-metal leak valve is replaced by an MFC and an all-metal valve.

Technical data
Filament type	DC heated low voltage filament
Gas line	filament heated cracking tube
Thermocouple	W5%Re/W26%Re (type C)
Bakeout temperature	250°C
Operating temperature	up to 1700ºC
Cooling	integrated water cooling
Accessories	aperture plate
	leak valve

Dimensions

Schematic drawing of the Oxygen Atom Beam Source OBS

(drawing shows OBS 40
with optional aperture and leak valve)

Specific data

For general information on CF mounting flanges see Flange and Gasket dimensions.


	[mm]	[mm] / [mm]	[W]	[A]	[V]
OBS	40-	L190-400 / D36	<200	< 15	< 15

***

specify UHV length L with order

Product code:

e.g. OBS 40-L220D36

is an oxygen atom beam source on DN40CF flange with UHV-length 220 mm and in-vacuum diameter 36 mm.

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OBS

Oxygen Atom Beam Source

Application

Gas Injection System

Technical data

Dimensions

Specific data

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