- Provides cracked or uncracked sulfur flux
- Suitable for other materials like Cs, Pb, K as well (m odifications on request)
- Flux modulation and on/off control by motorized valve
- Source capacities from 300 up to 9600 cm³
- Water-cooled assembly
- Excellent flux uniformity due to beam shaping nozzle
- Avoids loss of sulfur during system bakeout Datasheet
Introduction
The VCS is a valved sulfur cracker, employed in high efficiency CIS solar cell growth and other II-VI semiconductor material deposition applications.
Sulfur beam pressure is generated in a heated large capacity metal
crucible with inserted quartz liner. The sulfur flow rate is controlled
and switched on/off by a specially designed sulfur-resistant valve whose
outlet opens into an injection tube that includes an independently
heated cracking zone. The temperature within the cracking zone can be
adjusted to generate either uncracked or cracked sulfur. The use of a
beam shaping nozzle at the end of the injection tube provides excellent
flux uniformity on the substrate.
The valve design features a large cross-section orifice which allows
very good pumping properties of the reservoir. Its robust wide angle
valve design effectively eliminates the risk of locking, which is a
frequently observed problem with needle valves.
Technical details of the construction have been optimized to meet the specific requirements of research deposition applications and MBE systems. Simple system integration and excellent long-term run-to-run stability have been demonstrated. Different crucible sizes of 300 cm³ or 500 cm³ are offered on DN63CF (O.D. 4.5”).
For very large capacity industrial sources please see PVSS . The figure on the right-hand side shows an industrial version, applied in sulfurization processes in thin film solar cell manufacturing.
Application
The VCS Valved Sulfur Cracker Source has been designed for the controlled evaporation of sulfur. It can be used for II-VI semiconductor thin film research and solar cell manufacturing. Other possible applications are, for example, post-growth sulfurization processes.
MBE-Komponenten provides support in the design of customer-specific research or production systems in order to achieve a customized source geometry, optimized for specified layer uniformity and most efficient deposition material consumption.
Co-deposition processes can be simulated on request. The simulations are based on geometric and Monte Carlo method calculations. Typical results include the lateral layer thickness distribution and material composition for multiple material co-deposition processes on semiconductor wafers as well as on large area substrates.
Type | VCS-300 | VCS-500 |
Crucible capacity | 300 cm³ | 500 cm³ |
Length of injector tube | 250 to 400 mm | 250 to 400 mm |
In-Vacuum diameter (w/o cooling shroud) | see drawing below | contact us |
Operating temperatures - crucible zone - cracker (no cracking) - cracker (cracking) | 150 to 300°C 400°C 800-1000°C | 150 to 300°C 400°C 800-1000°C |
Outgassing temperature (crucible / cracker) | 300° / 1200°C | 300° / 1200°C |
Bakeout temperature | 250°C | 250°C |
Water cooling | main body injector tube (option) | main body injector tube (option) |
Valve opening time | 1 sec | 1 sec |
Heater circuits | - crucible + valve - cracker | - crucible + valve - cracker |
Thermocouples | W5%Re/W26%Re (typeC) 2 thermocouples (crucible-valve / cracker) | W5%Re/W26%Re (typeC) 2 thermocouples (crucible-valve / cracker) |
Valve control | manual or motor drive MVCU | manual or motor drive MVCU |